The pycnometer a glass flask whose inner volume can be very precisely determined and reproduced is a device used for measuring the gravimetric density. The liquids used in this work covers distilled water and various oil qualities as pure phases. The measurement and control of liquid density can be quite critical in industrial processes. This demonstration illustrates the methods for measuring the density of solids and liquids. Determining the density of liquids using the pycnometer. The measuring task is to determine the densities of waterethanol mixtures. Knowing the mass and volume of an object allows the calculation of its density. Jan 31, 2006 volume and density determination methods using manual laboratory devices. The density of a liquid can be determined by several methods. Fundamentals of natural gas liquid measurement don sextro targa resources louisiana, suite 4300 houston, texas 77002 dan comstock the university of texas petex 4702 n sam houston parkway w suite 800 houston, texas 77086 introduction the measurement of natural gas liquids ngl is similar.
Specimen volume cm3 mass grams density gmcm3 liquids density gcm3 mercury. In the following experiment, the identities of three colorless liquids will be determined by measuring the densities of the liquids by two methods and then comparing the density of the liquid to literature reference values for the three liquids. A noncontact measurement technique for the density and. A second method, called the bottle method, uses a specificgravity bottle, i. Measuring densities of solids and liquids using magnetic levitation. Density is the ratio of a substances mass to its own volume. Two methods are commonly used for determining the specific gravities of liquids. In the experiments to test lavit for measuring the interfacial tension between density matched liquids section 4. The density of a liquid is far easier to measure than that of a solid or gas. Using a pan balance, determine and record the mass of an object in grams. Measuring liquid density using archimedes principle iopscience.
Different methods of density measurement instrumentation. Acoustic measurement of liquid density with applications. It is dedicated to explaining what density is, how this parameter is defined and measured, the history of density measurement, the different methods available, and also how to ensure you get the best density result by using the techniques of good. The identity of an unknown metal will be established in a similar manner.
This guideline lists these methods, giving only a very succinct description of them, and the reader is referred to the standards which are listed in the appendix. Application of density meters to liquid hydrocarbon measurement. One method uses the hydrometer, an instrument that gives a specific gravity reading directly. The effect of acoustic diffraction is eliminated by using the. Its measure is usually given in grams g or kilograms kg. Pycnometry specific gravity bottles a pycnometer is. Capillary viscometer this method is based on using capillary tubes and the time it takes for a volume of l. Peffer density data may be used for obtaining relationships between density, chemical composition, thermal and mechanical treatments of materials, etc. At deep depths, porosity of geological formations can be evaluated based on well logged data. The best procedures for density determination of solids are the buoyancy and displacement methods, both based on. In static measurement methods, the liquid equivalent of the vapor space must be determined. The relative density of some common liquids as measured using the marble is shown in table 1.
Standard test method for density and relative density. In simple terms a measuring cylinder is sufficient for reasonable approximations. For example, the density of a gold coin and a gold statue are the same, even though the gold statue. The technique involves placing a container of the liquid under test on an. Density of solids and liquids by peter hidnert and elmer l. A special holder can also be used to measure density of solids. Determining the density of a solid and liquid protocol.
Homework statement i have to find two methods used to measure the density of a solid material and one method to measure a liquids density homework equations na the attempt at a solution got one method for the solids and have written this but my teacher wants me to find the. There are several experimental methods used for density determination of liquids. Although not a complete list, the following represents the most common methods by which volume and density are determined manually. A new approach to determine the density of liquids and solids. As for liquids, the measured density of a solid sample is the ratio of the measured mass to the. Measurement of density introduction in order to classify and. A second cylinder is placed in the center of the cup and the bob is shaped like an inverse cup that turns in the ringshaped gap between the cups. The cm3 volume unit used with solids is numerically equal to ml volume unit used with liquids. Using a volumetric flask and an analytical balance, the density of ethanol can be determined. The measurements can be made in liquids, stationary or in motion. For this reason it is the preferred method in case of disputes. The pyknometer is a pearshaped bottle in which the liquid to be investigated is filled for weighing. A method for determining the gas density, liquid density, and the volumetric flow rates of a multiphase fluid and each of the components of said multiphase fluid comprising a gas and a liquid mixture of oil and water without separating gas from said multiphase fluid, wherein the densities of the oil and water are known, the specific gravity of the gas is known, the pressure and temperature. There are numerous units for volume including liters l, meters cubed m3, and gallons gal.
Pycnometry specific gravity bottles a pycnometer is a vessel with a precisely known volume. Viscosity, in simple terms, is a fluids resistance to flow. Using this method, the density of any solids or liquids can be. A feedback circuit is described which varies the frequency of an oscillator producing the vibrations so as to. The frequency at which a resonance mode, usually a fundamental, is produced is a function of the density of the liquid. Feb 21, 2017 not such an easy question as first appears. The shear viscosity of most liquids decreases with temperature and increases with pressure, which is. This means that the value of density is independent of the quantity of matter present. Astm d1217 15 standard test method for density and. Volume and density determination methods using manual laboratory devices. Care must be taken to provide a representative sample of the flowing fluid where a density measurement is made. The density of a gas further depends on the pressure as well. Keep two stopwatches ready to measure the fall time between two different calibrated positions. Determining the density of a solid and liquid protocol jove.
Method of measuring the thermal conductivity of liquids 8 1 correction of the heat production in formula 3 with q qt. You can, however, measure the volume and mass of a liquid directly and, for most applications, simultaneously. Acoustic measurement of liquid density with applications for. Mass is a measure of the amount of matter an object has. D4052 test method for density, relative density, and api gravity of liquids by digital density meter. The difference between m1 and m2 buoyancy divided by the volume of the glass body is the density of the sample. Determine the density of an object with an irregular shape. In particular, because the most widely used of these methods, historically, has been the ring method. Density measurement of solid, liquid and viscous samples on an analytical or precision balance fast and easy process with density kit and balance application.
Volume and density definitions and determination methods. This paper presents two methods to measure the density of liquids based on the measurement of the reflection coefficient and propagation velocity, using a novel doubleelement transducer. Determine the densities of one solid material and one liquid. The main factors that affect the precision of the measurements are analyzed. The accuracy and precision of the density measurement expressed as a percentage of the absolute value is 0. The subject of this thesis is to investigate methods for measuring liquid density by acoustic means, and to investigate one or more promising methods experimentally. What methods are used to measure the volume of a liquid. The identity of an unknown metal will be established in. Methods used to measure the density of solid materials and. A method for measuring the interfacial tension for density. Standard test method for density, relative density, and. Robust and wellknown, pressure transmitters known as hydrostatic devices when measuring liquid level are the most common measuring device for liquid level in a tank. Ultrasonic measurement of density of liquids article pdf available in the journal of the acoustical society of america 971. Us5535632a systems and methods for measuring flow rates.
In the experiments to test lavit for measuring the interfacial tension between densitymatched liquids section 4. May 31, 2012 homework statement i have to find two methods used to measure the density of a solid material and one method to measure a liquids density homework equations na the attempt at a solution got one method for the solids and have written this but my teacher wants me to find the. The most important parts of measuring the density of a liquid are ensuring you calibrate the scale properly and read the volume accurately. Using a vernier caliper or ruler, measure the length, depth and width of the object in centimeters. Therefore if we want to get curve a from curve b we have to take a. A glass body of defined volume is weighed in air m1, dipped into the sample and weighed again in the sample m2. Measuring the volume the volume of an irregularly shaped object can be determined by measuring the amount. Calculate the density by measuring the mass and volume. This standard is based on the is0 758 method for determination of density of liquids at 20c.
A simple technique is described for measuring absolute and relative liquid density based on archimedes principle. Us5535632a systems and methods for measuring flow rates and. Amongst the four common methods available for determining the surface tension of liquids and solutions ring method, plate method, pendant drop, and bubble pressure method it worthwhile to note some differences in capabilities and limitations. Request pdf a new approach to determine the density of liquids and solids.
Jul 29, 2016 viscosity, in simple terms, is a fluids resistance to flow. Determine the density of an object with a regular shape. To determine the densities of water, an unknown liquid, a rubber stopper, and an unknown. The cup is not a hollow cylinder, nor is the measuring bob a solid body. D6809 guide for quality control and quality assurance procedures for aromatic hydrocarbons and related materials.
Note, from the table below, that the density of water is 1 g. Determining the density of liquids using the pycnometer after. The toluene proportion was increased in the mixture to obtain a density closer to that of water. Astm d891 18 standard test methods for specific gravity. The volume of a solid can be difficult to obtain, while the mass of a gas can rarely be measured directly. Density determination by pycnometer is a very precise method. This work was performed at the christian michelsen research as, cmr. This paper presents two methods to measure the density of liquids based on the measurement of the reflection coefficient and propagation velocity, using a novel double. Obtain a set of objects cube, cylinder, sphere, etc. Doublegap systems 14 are a special form of concentric cylinders, specially devised for measuring lowviscosity liquids.
Porosity, density, and permeability are all important parameters and properties to consider with regards to oil and gas industry. The pyknometer is a pearshaped bottle in which the liquid to be investig. You first weigh the empty flask and then the one filled with the liquid sample. Measuring the mass trial sample 1 sample 2 1 2 3 avg. A device for measuring the density of a liquid relies on the generation of resonant modes in a torsional vibration set up in a paddle which is immersed in the liquid. Density is defined as the mass divided by the volume of the object.
It depends on the liquid and how accurate the measurement. Bring the ball with a tweezers over the tube and drop it carefully into the liquid at the centre of the tube. When measuring liquids and regularly shaped solids, mass and volume can be discovered by direct measurement and these two measurements can then be used to determine density. Adjust the scale using manual adjustments or the scales automatic tare function, so the scale reads 0 with the container on it. Using a graduated cylinder, analytical balance, and water as the displaced liquid, the density of zinc metal can be determined. What are the different methods to measure the viscosity of. E1 specification for astm liquidinglass thermometers. This means that every centimeter cube of this wood will have a mass of 0. Different measuring techniques comparison for density and. This presentation will provide information about three approaches in common. Standard test method for density, relative density, and api.
It is the ratio of the density of a substance to the density of water, at a standard temperature. To determine the density of liquids, the pyknometer after gaylussac is used in the experiment p1. As the need for energy demands increase, deeper and newer extractions methods must be utilized to obtain fuel. Measuring densities of solids and liquids using magnetic. Use three methods to determine the volumes of solid aluminum and solid brass. We will learn how to use pycnometer in this assignment. However, they are more commonly used to measure flow rate of steam, gases or liquids, or the level of liquids in tanks.
The best procedures for density determination of solids are the buoyancy and displacement methods, both based on archimedes principle. Sniegoskichemical sciences divisionmaterial measurement laboratorynational institute of standards and technology1gaithersburg, md 20899the determination of solution density is required for conversion of liquid solution levels from a mass fraction basis to a volume fraction basis. Fundamentals of natural gas liquid measurement don sextro targa resources louisiana, suite 4300 houston, texas 77002. The units of density are commonly expressed as gcm 3 for solids, gml for liquids, and gl for gases. Mass should be expressed in units of grams and volume in units of ml or cm3.
Most methods for determining the density of liquids and solids are the object of national and international standardizing bodies and are frequently specified by governmental agencies. The focus of this page is on the density of fluids, meaning the density of liquids and gases. Calculate the density by measuring the mass and volume of your samples. Nevertheless, this effect is negligible in a case of liquid andor solid matter. Determine the density of a liquid calculate the density by measuring the mass and volume of your liquid sample. This circular defines density and specific gravity, describes 11 methods hydrostatic weighing, picnometer, flotation. Following are the various methods used to measure the viscosity of a fluid. Measuring density background all matter has mass and volume.
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